The REG Procedure

This example shows how you can use lack-of-fit tests with the REG procedure. See the section Testing for Lack of Fit for details about lack-of-fit tests.

In a study of the percentage of raw material that responds in a reaction, researchers identified the following five factors:

The following data set contains the results of an experiment designed to estimate main effects for all factors:

data reaction;
   input FeedRate Catalyst AgitRate Temperature
         Concentration ReactionPercentage;
   datalines;
10.0   1.0  100   140  6.0   37.5
10.0   1.0  120   180  3.0   28.5
10.0   2.0  100   180  3.0   40.4
10.0   2.0  120   140  6.0   48.2
15.0   1.0  100   180  6.0   50.7
15.0   1.0  120   140  3.0   28.9
15.0   2.0  100   140  3.0   43.5
15.0   2.0  120   180  6.0   64.5
12.5   1.5  110   160  4.5   39.0
12.5   1.5  110   160  4.5   40.3
12.5   1.5  110   160  4.5   38.7
12.5   1.5  110   160  4.5   39.7
;

The first eight runs of this experiment enable orthogonal estimation of the main effects for all factors. The last four comprise four replicates of the centerpoint.

The following statements fit a linear model. Because this experiment includes replications, you can test for lack of fit by using the LACKFIT option in the MODEL statement.

proc reg data=reaction;
   model  ReactionPercentage=FeedRate Catalyst AgitRate
                             Temperature Concentration / lackfit;
run;

Output 85.6.1 shows that the lack of fit for the linear model is significant, indicating that a more complex model is required. Models that include interactions should be investigated. In this case, this will require additional experimentation to obtain appropriate data for estimating the effects.